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Abstract: the transport properties are dominated by Josephson ﬂuxon ﬂow (for junctions whose dimensions exceed the Josephson penetration. depth) and premature switching to the voltage state at bias cur rents less than the critical current (for junctions whose dimen ...

IEEE TRANSACTIONS ON APPLIED SUPERCONDUCTIVITY, VOL. 15, NO. 2, JUNE 2005 237
Fabrication and Characterization of SubMicron Thin
Film Intrinsic Josephson Junction Arrays
P. A. Warburton, A. R. Kuzhakhmetov, G. Burnell, M. G. Blamire, Y. Koval, A. Franz, P. Müller, and H. Schneidewind
Abstract—We have fabricated intrinsic Josephson junction ar across the barrier is spatially uniform this dependence is of the
rays in thin ﬁlms of TlBaCaCuO. Such arrays are candidates form:
for applications in the submillimeter waveband both by virtue of
the large gap energy and due to the existence of inductive and
capacitive coupling mechanisms between junctions in the array.
(1)
Characterization of such junctions is complicated by the fact that
the transport properties are dominated by Josephson ﬂuxon ﬂow
(for junctions whose dimensions exceed the Josephson penetration
depth) and premature switching to the voltage state at bias cur where is the ﬁeld required to insert a ﬂux quantum into a
rents less than the critical current (for junctions whose dimen single junction. If, however, Josephson ﬂuxons are present in
sions are less than the Josephson penetration depth). Here we show the junction, the phase difference is highly spatially nonuniform,
that the magneticﬁeld dependence of the switching current is not leading to signiﬁcant deviations from the socalled Fraunhofer
Fraunhoferlike, although there is clear minimum corresponding
to the point at which a single ﬂux quantum is inserted between the dependence of (1) [6]. In zero ﬁeld such ﬂuxons are present for
cuprate doubleplanes. Nevertheless a Fraunhoferlike dependence junctions with linear dimension exceeding the Josephson pen
can be obtained if the critical current is experimentally deﬁned by etration depth, . Small junctions, on the other hand, are sus
specifying a lowvoltage criterion. ceptible to premature switching by thermal activation. Such pre
Index Terms—Josephson junctions, superconductivity, thermal mature switching occurs at a current, , which can be much
noise. less than , rendering direct measurements of the Fraunhofer
dependence impossible. As we will show below, for intrinsic
Josephson junctions there exists no junction size in which
I. INTRODUCTION
there is neither penetration of Josephson ﬂuxons nor premature
S INCE the spacing of consecutive copperoxide double
planes in many cuprate superconductors is greater than the
coherence length in the cdirection, such planes are Josephson
switching at 4.2 K. This suggests that measurements of
should never be Fraunhoferlike at 4.2 K. Nevertheless we ex
perimentally show that by deﬁning a critical current at an ar
coupled. Hence a cuprate superconductor which is structured in bitrary low voltage of order , a Fraunhoferlike dependence
such a way that the current is forced to ﬂow in the cdirection can be observed.
acts as a series array of “intrinsic” Josephson junctions [1].
Such junctions show promise for a wide variety of applications. II. ANALYSIS
For example, zerocrossing Shapiro steps at frequencies up to
2.5 THz have been measured in single crystal BiSrCaCuO Given that Josephson ﬂuxons must be excluded, the max
intrinsic junctions [2], suggesting that they are suitable for imum area of a junction in which one might expect to see
development as voltage standards and submmwave oscillators the Fraunhofer dependence is of order . The maximum
[3], [4]. A variety of thinﬁlmbased device geometries has Josephson energy of such a junction is thus
also been proposed, with a view to further exploiting intrinsic
Josephson effects in device applications; for a review of such (2)
devices see [5].
The conventional way to conﬁrm that Josephson coupling is where is the ﬂux quantum and the critical current density.
the transport mechanism in any novel type of Josephson device For intrinsic Josephson junctions, is given by [7]
is to measure the inplane magneticﬁeld dependence of the crit
ical current, . For a junction in which the phase difference (3)
Manuscript received October 5, 2004. This work was supported in part by the
U.K. Engineering and Physical Sciences Research Council. where is the permeability of free space, is the
P. A. Warburton and A. R. Kuzhakhmetov are with University College thickness of the cuprate doubleplanes, and is the inplane
London, Department of Electrical and Electronic Engineering, Torrington
Place, London, WC1E 7JE, U.K. (email: [email protected]).
penetration depth. By combining (2) and (3) we ﬁnd that the
G. Burnell and M. G. Blamire are with the University of Cambridge, Dept. of maximum Josephson energy for an intrinsic junction which can
Materials Science, Cambridge, CB2 3QZ, U.K. be expected to show the Fraunhofer dependence is
Y. Koval, A. Franz and P. Müller are with Universität ErlangenNürnberg,
Physikalisches Institut III, D91058, Erlangen, Germany.
H. Schneidewind is with IPHTJena, 07745 Jena, Germany. (4)
Digital Object Identiﬁer 10.1109/TASC.2005.849766
10518223/$20.00 © 2005 IEEE
238 IEEE TRANSACTIONS ON APPLIED SUPERCONDUCTIVITY, VOL. 15, NO. 2, JUNE 2005
Fig. 1. Schematic (not to scale) of our device geometry. The slanting lines in
H
the center of the structure indicate the orientation of the copperoxide double
planes. shows the magnetic ﬁeld vector and I the transport current. The
devices reported here are of length l = 3 m, width w = 0:5 m and ﬁlm
thickness b = 240 nm.
A Josephson junction switches to the voltage state by escape
out of a potential well of height
(5)
where is the normalized bias current [8]. Our model is
based upon the simplifying assumption that thermal activation
from this potential well occurs when , where is a
phenomenological factor of order 1 and is Boltzmann’s con
stant. (This approximation is only applicable in the limit
. A full and more precise model applicable for has
been published in [9].) Under this assumption the normalized
current at which switching to the voltage state occurs is given
by
(6)
Fig. 2. (a) Part of the currentvoltage characteristics of an intrinsic Josephson
By combining (4) and (6) we can now obtain the maximum junction array in zero magnetic ﬁeld at T = 4:2 K. Only ten of the quasiparticle
value of the normalized switching current for a Josephson junc branches are shown here. (b) Enlargement of the lowvoltage region of (a).
tion in which ﬂuxons are excluded. By putting
and we ﬁnd that at —i.e. in using argonion milling and submicron features using a 30
junctions in which we can expect the critical current to follow keV gallium focussed ionbeam.
the Fraunhofer dependence, the apparent critical current, , is Transport measurements in zero magnetic ﬁeld are performed
at most 68% of the actual critical current, , at the usual mea by immersing the sample into a liquid helium storage vessel.
surement temperature. Conversely, if we pose the question “at Measurements in a magnetic ﬁeld of up to 3 T are performed in
what temperature should measurements be made so that the ap an Oxford Instruments helium cryostat. The sample may be ro
parent critical current is within 5% is the actual critical current?” tated with respect to the ﬁeld with angular resolution better than
we ﬁnd an upper limit for this temperature to be 260 mK. 0.1 . This high precision allows us to avoid inserting pancake
vortices, for which it is essential that the misalignment between
III. EXPERIMENTAL the applied ﬁeld vector and the copperoxide planes be less than
, where is the lower critical ﬁeld of
Our device geometry which makes use of misaligned in the cdirection. For our maximum applied
ﬁlms is shown in Fig. 1. The substrate is ﬁeld of 3 T this implies that the misalignment must be smaller
vicinal lanthanum aluminate with its surface cut at an angle than . Details of the alignment procedure can be found
of 20 to the (0 0 1) axis. The ﬁlms, of thickness 240 nm are elsewhere [12].
grown by sputtering an amorphous BaCaCuO precursor and
ex situ annealing in a thallous atmosphere at around 800 IV. RESULTS
[10]. During the annealing process the TBCCO ﬁlm recrys
tallizes epitaxially on the vicinal substrate with the result that A. CurrentVoltage Characteristics
the copperoxide double planes are misaligned by 20 with The currentvoltage characteristics of a device of width
respect to the substrate surface. This epitaxy is conﬁrmed both are shown in Fig. 2. The characteristics are
by fourcircle xray diffraction and crosssectional transmission multibranched (in common with all intrinsic Josephson de
electron micrography [11]. Micronscale features are patterned vices), each branch corresponding to an additional junction
WARBURTON et al.: FABRICATION AND CHARACTERIZATION OF INTRINSIC JOSEPHSON JUNCTION ARRAYS 239
Fig. 3. Temperature dependence of the switching current in zero ﬁeld. The Fig. 4. Dependence of the switching current (circles) and critical current
points are the experimental data and the line is a ﬁt using the thermal activation (diamonds) upon an inplane aligned magnetic ﬁeld at T = 4:2 K, in both
model of equation (6). The ﬁtting parameter is = 0:8 (see text for details). cases normalized to their respective zeroﬁeld values. The critical current
is deﬁned at a voltage criterion of 5 V . The line shows the Fraunhofer
dependence (equation (1)) with H = 2:37 T as the ﬁtting parameter.
entering the voltage state. The reason for higher order branches
switching at lower apparent critical current values is not
understood. The supercurrent branch is not at zero voltage, that the Josephson phenomena we observe are indeed intrinsic
the dissipation here being due to thermallyactivated phase to the cuprate doubleplanes.
diffusion [12], [13]. The current at which the jump from the Nevertheless it is clear that the switching current dependence
supercurrent branch occurs (equal to 5.5 here) is therefore does not follow the Fraunhofer dependence, which is to be ex
not the Josephson critical current. We have previously shown pected given that thermal ﬂuctuations play a strong role in the
by studying the temperature dependence of the supercurrent switching process. We therefore also plot in Fig. 4 the mag
branch in this device that the zeroﬁeld lowtemperature critical neticﬁeld dependence of the critical current deﬁned at an ar
current is 7.2 [13], corresponding to a Josephson energy of bitrary voltage criterion of 5 . Here the data are normalized
K. This critical current, in common with BCS supercon to the zeroﬁeld value which is 190 nA. The ﬁt to the Fraunhofer
ductors, is approximately constant for temperatures less than dependence (1) suggests that this lowvoltage deﬁnition of the
half the superconducting transition temperature. critical current is a more accurate measure of the true critical
current than is the switching current. Care must therefore be
B. Temperature Dependence of the Switching Current taken in interpreting the criticalcurrent ﬁelddependence data
for all small intrinsic Josephson junctions at 4.2 K.
The temperature dependence of the switching current is
shown in Fig. 3, where we restrict ourselves to , in
which regime the critical current is essentially constant. We now V. CONCLUSIONS
use our simpliﬁed thermal activation model (6) to account for We have shown that due to premature switching it is not pos
the temperature dependence of . This dependence is shown sible to directly measure the Fraunhofer dependence of the crit
in Fig. 3, with as described in the previous ical current in intrinsic Josephson junctions at 4.2 K. We esti
section. The only ﬁtting parameter is the phenomenological mate an upper bound on the temperature for such measurements
term , which is 0.8 here. We conclude that, although the model to be successful to be 260 mK. We have further developed a
is clearly oversimpliﬁed, it is adequate for giving order of simpliﬁed model of thermallyactivated premature switching of
magnitude estimates for the degree to which measurements of Josephson junctions with . This model allows us to es
the switching current underestimate the critical current in small timate the magnitude by which measurements of the switching
intrinsic Josephson junctions with . current underestimate the critical current.
C. MagneticField Dependence of the Switching Current REFERENCES
The dependence of the switching current, normalized to its [1] R. Kleiner, F. Steinmeyer, G. Kunkel, and P. Mueller, “Intrinsic
zeroﬁeld value, upon an inplane aligned magnetic ﬁeld is Josephson effects in Bi2sr2cacu2o8 singlecrystals,” Phys. Rev. Lett.,
vol. 68, p. 2394, 1992.
shown in Fig. 4. There is a clear minimum at . [2] H. B. Wang, P. H. Wu, and T. Yamashita, “Terahertz responses of in
The ﬁeld required to insert a single ﬂux quantum per intrinsic trinsic Josephson junctions in high Tc superconductors,” Phys. Rev. Lett.,
junction is given by [7] vol. 87, p. 107 002, 2001.
[3] M. Bae, H. Lee, J. Kim, and K. Kim, “Microwave distribution in stacked
Bi2Sr2CaCu2O8+x intrinsic Josephson junctions in a transmissionline
(7) geometry,” Appl. Phys. Lett., vol. 83, p. 2187, 2003.
[4] H. Wang, J. Chen, P. Wu, T. Yamashita, D. Vasyukov, and P. Muller,
where is the separation of the cuprate doubleplanes. Inserting “Intrinsic Josephson junctions: integrated circuits and possible applica
tions,” Supercond. Sci. Technol., vol. 16, p. 1375, 2003.
the appropriate values for this device we ﬁnd , in [5] A. A. Yurgens, “Intrinsic Josephson junctions: recent developments,”
reasonable agreement with the measured minimum, conﬁrming Supercond. Sci. Technol., vol. 13, p. R85, 2000.
240 IEEE TRANSACTIONS ON APPLIED SUPERCONDUCTIVITY, VOL. 15, NO. 2, JUNE 2005
[6] A. Barone and G. Paterno, Physics and Applications of the Josephson [11] O. S. Chana, A. R. Kuzhakhmetov, D. M. C. Hyland, C. J. Eastell, D.
Effect. New York: Wiley, 1988. DewHughes, C. R. M. Grovenor, Y. Koval, M. Moessle, R. Kleiner,
[7] R. Kleiner and P. Müller, “Intrinsic Josephson effects in highTc super P. Müller, and P. A. Warburton, “Fabrication and measurement of in
conductors,” Phys. Rev. B, vol. 49, p. 1327, 1994. trinsic Josephson junctions in misaligned ﬁlms of Tl2Ba2CaCu2O8.,”
[8] M. Tinkham, Introduction to Superconductivity, 2nd ed. New York: IEEE Trans. Appl. Supercond., vol. 11, p. 2711, 2001.
McGrawHill, 1996. [12] P. Warburton, A. Kuzhakhmetov, O. Chana, G. Burnell, M. Blamire,
[9] A. Franz, Y. Koval, D. Vasyukov, P. Muller, H. Schneidewind, D. A. H. Schneidewind, Y. Koval, A. Franz, P. Muller, D. Hyland, D. Dew
Ryndyk, J. Keller, and C. Helm, “Thermal ﬂuctuations in ultrasmall in Hughes, H. Wu, and C. Grovenor, “Josephson ﬂuxon ﬂow and phase
trinsic Josephson junctions,” Phys. Rev. B, vol. 69, p. 014 506, 2004. diffusion in thinﬁlm intrinsic Josephson junctions,” J. Appl. Phys., vol.
[10] H. Schneidewind, M. Manzel, G. Bruchlos, and K. Kirsch, “Tl 95, p. 4941, 2004.
BaCaCuO(2212) thin ﬁlms on lanthanum aluminate and sapphire [13] P. A. Warburton, A. R. Kuzhakhmetov, G. Burnell, M. G. Blamire, and
substrates for microwave ﬁlters,” Supercond. Sci. Technol., vol. 14, p. H. Schneidewind, “Decoupling of a small currentbiased Josephson
200, 2001. junction from its environment,” Phys. Rev. B, vol. 67, p. 184 513, 2003.
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